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In the current study, we apply a plethora of techniques, including NMR, HDX-MS, and native nano electrospray ionisation (ESI) MS to study the differences in the conformation of aggregation prone and non-aggregation prone monomeric aSyn including phosphorylated aSyn, pS129, and familial aSyn mutants, A30P, E46K, H50Q, G51D, A53T and A53E